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ANALYTICAL CHEMISTRY |
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Class Hours: 3.0 |
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Credit Hours: 4.0 |
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Laboratory Hours: 5.0 |
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Revised: Fall 2006 |
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Catalog Course
Description: |
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Principles and practices of
quantitative measurements in chemical systems are introduced. Chemical equilibria (acid-base, complexometric,
and redox), elementary pectrophotometry, chemical
separations--including chromatography, ion exchange, and solvent extraction--
are discussed. Course includes 3 hours of lecture and 5 hours of
laboratory applications each week. |
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Entry Level Standards: |
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One year of general
college chemistry is necessary for entrance into the course. |
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Prerequisite: |
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CHEM 1120 |
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Textbook(s) and Other
Course Materials: |
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Harris, Daniel C. Quantitative
Chemical Analysis, 7th edition. W. H. Freeman and Company, 2007. |
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I. Week/Unit/Topic
Basis: |
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Week |
Topic |
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1 |
Measurements; Tools of the
trade |
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2 |
Experimental error;
Statistics |
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3 |
Calibration methods |
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4 |
Chemical equilibrium |
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5 |
Titrations |
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6 |
Ionic strength; Activity
coefficients |
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7 |
Monoprotic and Polyprotic acid-base equilibria |
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8 |
Acid-base titrations |
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9 |
Fundamentals of
electrochemist |
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10 |
Fundamentals and
Applications of spectrophotometry |
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11 |
Acid-base titrations |
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12 |
Introduction to analytical
separations |
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13 |
Gas chromatography |
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14 |
High performance liquid
chromatography |
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15 |
Final Exam |
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II. Course Objectives*: |
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A. |
Follow written analytical
procedures and write lab reports understandable to others. VI.1. |
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B. |
Understand the underlying
principles of statistics in both lecture and lab. VI.1. |
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C. |
Understand chemical equilibria. I.5. |
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D. |
Understand ionic equilibria. I.5. |
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E. |
Understand the principles
of spectrophotometry and solve problems involving
light absorption and emission. III.1, III.2. |
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F. |
Solve problems dealing with
the principles of electrochemistry. I.5. |
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G. |
Calculate efficiencies of
separation for solvent extraction and chromatographic processes. I.5. |
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*Roman numerals after
course objectives reference TBR’s general
education goals. |
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III. Instructional
Processes*: |
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Students will: |
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1. |
Generate analytical data
within acceptable limits of experimental error. Technological Literacy
Outcome, Mathematics Outcome, Natural Sciences Outcome |
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2. |
Become proficient in
classical and instrumental methods of quantitative chemical analysis common
to modern analytical laboratories. Technological Literacy Outcome,
Transitional Strategy, Natural Sciences Outcome |
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3. |
Utilize current chemical
reference literature. Communication Outcome, Natural Sciences Outcome,
Technological Literacy Outcome |
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4. |
Record experimental data
and conclusions in a laboratory notebook in a manner acceptable for research and industry. Communication
Outcome, Transitional Strategy, Natural Sciences Outcome |
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5. |
Determine appropriate
method of chemical analysis for a substance based upon certain various
physical and chemical parameters. Technological Literacy Outcome, ActiveLearning Outcome |
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6. |
Understand the theories and
principles which underlie observed chemical processes. Communication
Outcome, Mathematics Outcome, Natural Sciences Outcome |
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*Strategies and outcomes
listed after instructional processes reference TBR’s
goals for strengthening general education knowledge and skills, connecting
coursework to experiences beyond the classroom, and encouraging students to
take active and responsible roles in the educational process. |
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IV. Expectations for
Student Performance*: |
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Upon successful completion
of this course, the student should be able to: |
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1. |
Understand the use and
calibration of lab equipment. A |
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2. |
Prepare a lab notebook for
data collection and reference. A |
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3. |
Understand how solutions
are prepared and work solution problems involving dilutions. A |
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4. |
Understand the safe
handling of chemicals and disposal methods of chemical wastes. A |
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5. |
Work solution problems
using the various concentration expressions. B |
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6. |
Convert given measurements
to necessary units needed in solving a particular problem. B |
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Understand the concept of
significant figures and perform mathematical operations with them. B |
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8. |
Distinguish between the
different types of experimental error. B |
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9. |
Estimate the uncertainty in
measurements. B |
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10. |
Determine and understand
the statistical analysis of experimental data. B |
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11. |
Understand the concepts
involving the chemical equilibrium constant, K. C |
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12. |
Review acid-base concepts
like strength, pH and use of ionization constants. C |
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13. |
Determine and use the
solubility product constant, Ksp, and the effects
of complex ion formation. D |
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14. |
Understand spectrophotometric concepts like absorbance,
transmittance, and Beer's Law, and gain experience with these concepts using
instrumentation. E |
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15. |
Review the technique of
titration and learn a variety of methods to determine information about the analyte. C,D,E,F |
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16. |
Review the concepts of
electrochemistry and extract chemical information using potentiometry.
F |
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17. |
Study two means of
analytical separations - extraction and chromatography. G |
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*Letters after performance
expectations reference the course objectives listed above. |
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V. Evaluation: |
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A. Testing Procedures: 50%
of grade |
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4 tests(100 points each) Final exam(100 points) Problems sets(25 points
each) Problem sets and exams may
not be made up if missed. The Final Exam may be worth more for an
excused missed exam. One lab grade may be dropped if all labs are
completed. |
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B. Laboratory Expectations:
50% of grade |
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Lab notebook - accuracy of
results and experimental write-up. Attendance is required for
scheduled lab meetings. All labs must be completed by the end of the
last scheduled lab meeting. Lab notebooks will be collected at this
meeting. See lab schedule for order of lab experiments and dates of lab
meetings. |
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C. Field Work: |
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N/A |
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D. Other Evaluation
Methods: |
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N/A |
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E. Grading Scale: |
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90-100
A |
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VI. Policies: |
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A. Attendance Policy: |
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B.
Academic Dishonesty: |
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With
any form of valid proof of dishonesty with regard to student work or testing,
the instructor may elect from a range of actions. Academic misconduct could
lead to failure for the assignment, and/or the entire course on consultation
with the program coordinator and Department Head. Additionally,
dismissal from the institution is an option and may be sought. |
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C. Accommodations for
disabilities: |
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If you need accommodations
because of a disability, if you have emergency medical information to share,
or if you need special arrangements in case the building must be evacuated,
please inform the instructor immediately. Please see the instructor privately
after class or in his/her office. Students must present a current
accommodation plan from a staff member in Services for Students with
Disabilities (SSWD) in order to receive accommodations in this course.
Services for Students with Disabilities may be contacted by going to Goins 127 or 131 or by phone: 694-6751(Voice/TTY) or
539-7153. |
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Posted:
September 21, 2006